Liquid secondary ion mass spectral study of fatty acid methyl esters: silver cationization and collision induced dissociation studies

1997 ◽  
Vol 11 (18) ◽  
pp. 1939-1944 ◽  
Author(s):  
K. Suma ◽  
N. Prasada Raju ◽  
M. Vairamani
Keyword(s):  
Fatty Acid ◽  
Spectral Study ◽  
Fatty Acid Methyl Esters ◽  
Methyl Esters ◽  
Collision Induced Dissociation ◽  
Mass Spectral ◽  
Acid Methyl ◽  
Mass Spectral Study ◽  
Secondary Ion

scholarly journals Studies in Improvement of Official Method 996.06

1999 ◽  
Vol 82 (5) ◽  
pp. 1146-1155 ◽  
Author(s):  
Jonathan W DeVries ◽  
Lori Kjos ◽  
Linda Groff ◽  
Martin Bob ◽  
Cernohous Kristi ◽  
...  
Keyword(s):  
Fatty Acid ◽  
Fatty Acid Methyl Esters ◽  
Methyl Esters ◽  
Official Method ◽  
Mass Spectral Data ◽  
Response Factors ◽  
Mass Spectral ◽  
Acid Methyl ◽  
Aoac Official ◽  
Aoac Official Method

Abstract Quantitation of fat in foods has been performed successfully with AOAC Official Method 996.06. A number of situations have been encountered that render the method note, “Note: For any unknown or uncalibrated peaks, use the nearest calibrated fatty acid response factors and conversion factors,” inaccurate. Identification of extraneous compounds and availability of additional standard fatty acid methyl esters combined with mass spectral data lead to the recommendation of modifications in Official Method 996.06. The stepwise performance of the method remains unchanged.

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